I used about 2 cups of bleach in a 20 gallon tub. Left it sit for 2 or 3 days.
Soaked in regular changes of fresh water (hose water).
Take a box of baking soda, bake it at 300 for an hour. It drives off the CO2. Sprinkle the rock with the baking soda, then dump it into the water. Not sure why I did this, except that it was easier than using a blow torch, which I considered. The harsh chemical reaction should burn off anything that is left, and it's harmless in the tank (within reason).
Bill
215g FOWLR... and anemones, GSP, gorgonians... carp, that isn't FO!
"I killed my first SW Fish in 1971..."